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Material Characterization and Replication

• • On site sampling of representative substrates and surface finishes
• • Microscopic examination, gravimetric analysis and chemical spot testing of samples
• • Coordination & interpretation of material analyses including: polarized light microscopy, fluorescence microscopy, infrared microscopy, scanning electron microscopy, and x-ray energy-dispersive spectrometry
• • Development of replication mixes of several historic finishes

Material characterization of over one hundred samples was performed for the overall documentation and interpretation of the masonry which makes up the Spanish Colonial Walls of Old San Juan, Puerto Rico. Many portions of these walls were constructed of tabby, an early version of cement.

ICR then conducted microscopic examination, gravimetric analysis, and chemical spot testing of samples and coordinated and interpreted material anlayses: polarized light microscopy, fluorescence and infrared microscopy, and SEM-EDX. 

The information gained from the materials analysis was used to create compatible replication mixes of the different historic stuccos and cement types for use as repair materials in future conservation campaigns. In-situ mock-ups were conducted to test the field performance of the replication materials. The laboratory mixes were then adjusted to compensate for differences in materials used and site conditions. Application techniques were also tested so final conservation materials and methods could be developed.